TA Instruments

AR1756-0003f

15/03/2013 14:47:32

Sample name	ASW Blank coupon#20 + DI + beads 150rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	3 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:47:32

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 150.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0160	129.7	658.62	10000	20.0	0.1522	1.016	214.7	162.1	1.324	620.0	102.3390	0.02360	127.92	12792	3.411E-3	0.0	0.0
2.0120	150.0	219.36	10000	20.0	0.1422	2.012	71.50	187.5	0.3814	579.5	291.3840	0.01649	364.23	36423	3.411E-3	0.0	0.0
3.0160	150.0	219.58	10000	20.0	0.1392	3.016	71.57	187.5	0.3817	567.1	417.1080	0.01613	521.39	52139	3.411E-3	0.1	0.1
4.0000	150.0	218.22	10000	20.0	0.1416	4.000	71.13	187.5	0.3793	577.0	542.0300	0.01641	677.54	67754	3.411E-3	0.1	0.1
5.0200	150.0	219.55	10000	20.0	0.1363	5.020	71.56	187.5	0.3817	555.5	731.8100	0.01580	914.76	91476	3.411E-3	0.1	0.1
6.0160	150.0	218.40	10000	20.0	0.1384	6.016	71.19	187.5	0.3797	563.8	856.1470	0.01604	1070.2	1.0702E5	3.411E-3	0.1	0.1
7.0160	150.0	216.35	10000	20.0	0.1380	7.016	70.52	187.5	0.3761	562.1	1044.7400	0.01599	1305.9	1.3059E5	3.411E-3	0.1	0.1
8.0160	150.0	214.88	10000	20.0	0.1400	8.016	70.04	187.5	0.3735	570.4	1170.5000	0.01622	1463.1	1.4631E5	3.411E-3	0.1	0.1
9.0200	150.0	213.82	10000	20.0	0.1382	9.020	69.70	187.5	0.3717	563.0	1296.0100	0.01601	1620.0	1.6200E5	3.411E-3	0.2	0.2
10.016	150.0	214.64	10000	20.0	0.1416	10.016	69.96	187.5	0.3731	577.0	1484.4800	0.01641	1855.6	1.8556E5	3.411E-3	0.2	0.2
11.016	150.0	213.58	10000	20.0	0.1390	11.016	69.62	187.5	0.3713	566.3	1610.2500	0.01611	2012.8	2.0128E5	3.411E-3	0.2	0.2
12.012	150.0	214.33	10000	20.0	0.1386	12.012	69.86	187.5	0.3726	564.6	1799.8300	0.01606	2249.8	2.2498E5	3.411E-3	0.2	0.2
13.016	150.0	213.61	10000	20.0	0.1386	13.016	69.62	187.5	0.3713	564.6	1924.6100	0.01606	2405.8	2.4058E5	3.411E-3	0.2	0.2
14.012	150.0	212.91	10000	20.0	0.1424	14.012	69.40	187.5	0.3701	580.3	2049.9700	0.01651	2562.5	2.5625E5	3.411E-3	0.2	0.2
15.016	150.0	211.08	10000	20.0	0.1363	15.016	68.80	187.5	0.3669	555.5	2239.8601	0.01580	2799.8	2.7998E5	3.411E-3	0.3	0.3
16.008	150.0	214.40	10000	20.0	0.1406	16.008	69.88	187.5	0.3727	572.9	2364.8101	0.01630	2956.0	2.9560E5	3.411E-3	0.3	0.3
17.012	150.0	211.86	10000	20.0	0.1382	17.012	69.06	187.5	0.3683	563.0	2489.8101	0.01601	3112.3	3.1123E5	3.411E-3	0.3	0.3
18.000	150.0	209.14	10000	20.0	0.1406	18.000	68.17	187.5	0.3636	572.9	2678.9600	0.01629	3348.7	3.3487E5	3.411E-3	0.3	0.3
19.000	150.0	214.02	10000	20.0	0.1414	19.000	69.76	187.5	0.3721	576.2	2804.0100	0.01639	3505.0	3.5050E5	3.411E-3	0.3	0.3
20.020	150.0	212.97	10000	20.0	0.1390	20.020	69.42	187.5	0.3702	566.3	2992.4600	0.01611	3740.6	3.7406E5	3.411E-3	0.3	0.3
21.016	150.0	210.50	10000	20.0	0.1400	21.016	68.61	187.5	0.3659	570.4	3119.0500	0.01622	3898.8	3.8988E5	3.411E-3	0.4	0.4
22.016	150.0	213.43	10000	20.0	0.1376	22.016	69.57	187.5	0.3710	560.5	3244.4399	0.01594	4055.6	4.0556E5	3.411E-3	0.4	0.4
23.016	150.0	212.89	10000	20.0	0.1382	23.016	69.39	187.5	0.3701	563.0	3433.9800	0.01601	4292.5	4.2925E5	3.411E-3	0.4	0.4
24.016	150.0	211.90	10000	20.0	0.1378	24.016	69.07	187.5	0.3684	561.3	3558.8201	0.01597	4448.5	4.4485E5	3.411E-3	0.4	0.4
25.016	150.0	209.34	10000	20.0	0.1404	25.016	68.23	187.5	0.3639	572.0	3746.4900	0.01627	4683.1	4.6831E5	3.411E-3	0.4	0.4
26.012	150.0	210.10	10000	20.0	0.1416	26.012	68.48	187.5	0.3652	577.0	3874.1299	0.01641	4842.7	4.8427E5	3.411E-3	0.4	0.4
27.012	150.0	209.45	10000	20.0	0.1386	27.012	68.27	187.5	0.3641	564.6	3997.7900	0.01606	4997.2	4.9972E5	3.411E-3	0.5	0.5
28.012	150.0	209.83	10000	20.0	0.1396	28.012	68.40	187.5	0.3648	568.7	4186.2700	0.01618	5232.8	5.2328E5	3.411E-3	0.5	0.5
29.016	150.0	208.97	10000	20.0	0.1390	29.016	68.11	187.5	0.3633	566.3	4311.9600	0.01611	5390.0	5.3900E5	3.411E-3	0.5	0.5
30.016	150.0	209.23	10000	20.0	0.1353	30.016	68.20	187.5	0.3637	551.4	4501.6401	0.01568	5627.1	5.6271E5	3.411E-3	0.5	0.5
31.016	150.0	211.20	10000	20.0	0.1406	31.016	68.84	187.5	0.3672	572.9	4627.4800	0.01629	5784.4	5.7844E5	3.411E-3	0.5	0.5
32.000	150.0	210.32	10000	20.0	0.1384	32.000	68.55	187.5	0.3656	563.8	4751.7998	0.01604	5939.8	5.9398E5	3.411E-3	0.5	0.5
33.012	150.0	214.91	10000	20.0	0.1376	33.012	70.05	187.5	0.3736	560.5	4940.3198	0.01594	6175.4	6.1754E5	3.411E-3	0.6	0.6
34.016	150.0	215.25	10000	20.0	0.1365	34.016	70.16	187.5	0.3742	556.3	5073.2202	0.01582	6341.5	6.3415E5	3.411E-3	0.6	0.6
35.016	150.0	211.56	10000	20.0	0.1386	35.016	68.96	187.5	0.3678	564.6	5191.7002	0.01606	6489.6	6.4896E5	3.411E-3	0.6	0.6
36.016	150.0	213.69	10000	20.0	0.1412	36.016	69.65	187.5	0.3715	575.3	5380.1299	0.01637	6725.2	6.7252E5	3.411E-3	0.6	0.6
37.016	150.0	211.97	10000	20.0	0.1402	37.016	69.09	187.5	0.3685	571.2	5505.7798	0.01625	6882.2	6.8822E5	3.411E-3	0.6	0.6
38.000	150.0	213.09	10000	20.0	0.1365	38.000	69.45	187.5	0.3704	556.3	5694.2598	0.01582	7117.8	7.1178E5	3.411E-3	0.6	0.6
39.016	150.0	211.16	10000	20.0	0.1378	39.016	68.83	187.5	0.3671	561.3	5820.3398	0.01596	7275.4	7.2754E5	3.411E-3	0.7	0.7
40.016	150.0	210.93	10000	20.0	0.1406	40.016	68.75	187.5	0.3667	572.9	5945.6299	0.01629	7432.0	7.4320E5	3.411E-3	0.7	0.7
41.016	150.0	212.23	10000	20.0	0.1416	41.016	69.18	187.5	0.3689	577.0	6134.6899	0.01641	7668.4	7.6684E5	3.411E-3	0.7	0.7
42.016	150.0	210.95	10000	20.0	0.1394	42.016	68.76	187.5	0.3667	567.9	6261.1802	0.01615	7826.5	7.8265E5	3.411E-3	0.7	0.7
43.016	150.0	211.27	10000	20.0	0.1398	43.016	68.86	187.5	0.3673	569.6	6449.4902	0.01620	8061.9	8.0619E5	3.411E-3	0.7	0.7
44.016	150.0	212.24	10000	20.0	0.1432	44.016	69.18	187.5	0.3690	583.6	6573.8599	0.01660	8217.3	8.2173E5	3.411E-3	0.7	0.7
45.016	150.0	210.43	10000	20.0	0.1400	45.016	68.59	187.5	0.3658	570.4	6699.7002	0.01622	8374.6	8.3746E5	3.411E-3	0.8	0.8
46.016	150.0	214.08	10000	20.0	0.1426	46.016	69.78	187.5	0.3722	581.1	6888.0400	0.01653	8610.1	8.6101E5	3.411E-3	0.8	0.8
47.016	150.0	212.33	10000	20.0	0.1380	47.016	69.21	187.5	0.3691	562.1	7013.7300	0.01599	8767.2	8.7672E5	3.411E-3	0.8	0.8
48.020	150.0	211.61	10000	20.0	0.1422	48.020	68.97	187.5	0.3679	579.5	7139.6099	0.01648	8924.5	8.9245E5	3.411E-3	0.8	0.8
49.020	150.0	211.10	10000	20.0	0.1378	49.020	68.81	187.5	0.3670	561.3	7328.1802	0.01597	9160.2	9.1602E5	3.411E-3	0.8	0.8
50.016	150.0	212.10	10000	20.0	0.1370	50.016	69.13	187.5	0.3687	558.0	7453.5098	0.01587	9316.9	9.3169E5	3.411E-3	0.8	0.8
51.016	150.0	212.16	10000	20.0	0.1402	51.016	69.15	187.5	0.3688	571.2	7642.0698	0.01625	9552.6	9.5526E5	3.411E-3	0.9	0.9
52.016	150.0	210.65	10000	20.0	-0.05600	52.016	68.66	187.5	0.3662	-228.2	7768.5698	-6.490E-3	9710.7	9.7107E5	3.411E-3	0.9	0.9
53.016	150.0	214.45	10000	20.0	0.1341	53.016	69.90	187.5	0.3728	546.4	7893.3901	0.01554	9866.7	9.8667E5	3.411E-3	0.9	0.9
54.044	150.0	210.77	10000	20.0	0.2814	54.044	68.70	187.5	0.3664	1147	8081.8198	0.03261	10102	1.0102E6	3.411E-3	0.9	0.9
55.012	150.0	212.28	10000	20.0	0.1355	55.012	69.19	187.5	0.3690	552.2	8207.5703	0.01571	10259	1.0259E6	3.411E-3	0.9	0.9
56.016	150.0	212.10	10000	20.0	0.02191	56.016	69.13	187.5	0.3687	89.28	8396.0303	2.539E-3	10495	1.0495E6	3.411E-3	0.9	0.9
57.012	150.0	211.08	10000	20.0	0.1392	57.012	68.80	187.5	0.3669	567.1	8522.7900	0.01613	10653	1.0653E6	3.411E-3	1.0	1.0
58.012	150.0	208.69	10000	20.0	0.1365	58.012	68.02	187.5	0.3628	556.3	8647.3398	0.01583	10809	1.0809E6	3.411E-3	1.0	1.0
59.012	150.0	210.68	10000	20.0	0.1372	59.012	68.67	187.5	0.3662	558.8	8835.9297	0.01589	11045	1.1045E6	3.411E-3	1.0	1.0
60.012	150.0	211.42	10000	20.0	0.7280	60.012	68.91	187.5	0.3675	2966	8961.6299	0.08437	11202	1.1202E6	3.411E-3	1.0	1.0

